坩埚损坏分析(The possible reason for the crucible damaging ) 裂纹 ① 将常温状态下的坩埚直接放入高温中,或者直接快速加热。 ② 硬物撞击造成。 ③ 坩埚内积累了太多的炉渣。 ④ 金属液体没有清理干净,加热后胀破。 ⑤ 火焰控制不好,坩埚加热时受热不均匀,上下温度差大。 ⑥ 坩埚钳夹取的位置过于靠上,用力过大。 ⑦ 炉沿盖压得太紧或者坩埚上沿氧化严重。 ⑧ 将料锭 横向放入坩埚内,没有足够的膨胀 空间,胀破坩埚。 ⑨ 将热坩埚放在冷地面上,或者坩埚底座太小,不平整。 Cracking ① The crucible was not preheated or heated up too fast. ② The crucible was impacted by hard goods. ③ Too much slag left in the crucible. ④ The crucible was broken up by the melting metal left. ⑤ Uneven heating as a result of the bad flame controlling,which lead to much temperature difference between the top and the bottom for the crucible. ⑥ The contact position of the crucible and the crucible clamp was not proper or the force the between them was too big. ⑦ Too tighten for the furnace lid on the crucible or the crucible top oxidized seriously. ⑧ No enough space left when the ingot was putted into the crucible transversely. ⑨ The heated crucible was put on the cool base directly or the base was too small and irregular. 破洞和小孔 ① 硬物撞击造成,例如料锭扔入坩埚内或者清理坩埚时硬物冲击造成。 ② 溶剂直接加入到坩埚内壁上。 ③ 烘烤产生微小裂纹造成。 The broken hole and eye ① Impacted by the hard materials.For example,impacted by the hard materials during the cleaning process or the ingot was throwing into the crucible. ② The crucible inwall was covered by the solvent. ③ The appearance of the microcrack during the baking process. 腐蚀 ① 熔剂加入量,还有就是熔剂必须在金属熔化后加入。 ② 使用劣质焦炭或者炉渣所引起。 ③ 加入强腐蚀行性的添加剂。 Corrosion ① The solvent mass or it was added into the crucible before the metal melting. ② Coke oof poor quality or the slag. ③ Addition of highly corrosivesolvent.